ASBC Laboratory Proficiency Program
What is the ASBC Laboratory Proficiency Program?
The ASBC Laboratory Proficiency Program (LPP) is an important quality tool for laboratories testing brewing raw materials and the final brewed products. The program is an excellent way to validate a subscriber's measurement process. This enables subscribers worldwide to assess and strengthen their quality standards by evaluating the accuracy and consistency of their results.
ASBC recognizes the need for a service by which laboratories can check their procedures and compare results with peer laboratories on a regular basis. LPP offers a variety of beer, hops, malted barley, and barley samples that enable brewing and malting laboratories to:
- Routinely evaluate instrument performance
- Monitor the use of correct analytical techniques by laboratory personnel
- Identify opportunities to improve the quality of laboratory results
- Verify the reliability and accuracy of contract laboratories
Available Samples
The ASBC Laboratory Proficiency Program includes 5 sample types which you can learn more about below:
Ready to Subscribe?
Reference Standards and Gauges must now be purchased via the ASBC store. These items were previously available via the LPP order form.
Already Subscribed?
Questions?
Contact us at [email protected].
ASBC Laboratory Proficiency Program FAQ
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Participants subscribe to a series within Beer Analysis, Hops, Barley, and Malted Barley. Subscribers receive specially prepared samples according to the schedule specified for that subscription. Upon receiving the sample, analyses are conducted and results are submitted by the scheduled deadline through the subscriber portal. Complete confidentiality of results is guaranteed as each subscriber receives a unique ID that is updated on a yearly basis. Results are analyzed, and a report is issued containing the statistical analysis of the results submitted by all participating subscribers. Subscribers will also receive quantitative estimates of the accuracy of their submitted results. Fees vary depending upon the series, the frequency, and the subscriber's location.
Final LPP reports will be available within days of the deadline for reporting results. Series will require more than 6 data points or participants to generate Z-scores and kernel density graphs. The reports will identify the following:
- Series name, sample number and test material, and number of series participants.
- Participant reported data listed according to the subscriber unique ID.
- Assigned value (mean) and standard deviation for each constituent are reported after removal of data qualified as Grubbs' outliers.
- Z-scores (note: Z-scores are not calculated for data points classified as an outlier or for series having less than 6 participants.)
- Outliers as determined by the Grubbs' calculation (ISO 5725 Part 2) are noted on data entry reports with a G.
- Chart of Z-score plots the Z-scores according to subscriber unique ID. Z-scores greater than 2 standard deviations (S.D.) are indicated in yellow, greater than 3 S.D. are indicated in red.
- Kernel density plots show the raw data against the probability density. Raw data of greater than 2 S.D. are indicated by the yellow bar. Raw data greater than 3 S.D. values are indicated by the red bar.
Cancellation Policy
All cancellation requests must be submitted in writing. A cancellation request is made when a subscriber no longer wishes to receive samples or reports.
Cancellation requests must be made at least 45 days in advance of the "Portal Open Date" of the nearest round. Cancellation requests made within 45 days will be applicable to the following scheduled round.
Refunds will be granted only for pre-paid shipping fees and will be processed within 60 days of cancellation. No refunds will be granted for pre-paid series subscriptions. Extenuating circumstances will be evaluated on a case-by-case basis.
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The ASBC Laboratory Proficiency Program provides subscribers an opportunity to evaluate accuracy, as well as instrument performance on a regular basis. By comparing internal laboratory data to results from other laboratories around the world, a critical assessment of the analytical data generated by subscribing laboratories can be made. Subscribers can also build confidence in the analytical data generated by their laboratory personnel. Participating laboratories rely on proficiency programs for a number of reasons, including:
- Comparison of subscriber results with those of other peer laboratories over time (results are anonymous)
- Confirming analytical proficiency of laboratory personnel within the same facility or across multiple sites
- Benchmarking of best practices
- Qualification of contract laboratories
- Evaluation of alternative analytical methodologies
- Enhancement of process control capabilities by providing an independent means to assure gauge-related contributions to data variability
- Ensure accuracy of labeling information
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If measurements are made on beer or raw materials, the ASBC Laboratory Proficiency Program can help confirm the accuracy of those results for any sized operation!
Check out our other resources on Growing your Own Beer Quality Lab!
Available Samples
Beer Analysis
On a quarterly basis, subscribers receive a shipment of samples from a uniform lot of beer.
Subscribers to the Beer Analysis may add B or C to receive additional 6-packs.
Series
Beer Analysis 108A
One six-sample pack (bottles or cans) shipped quarterly
Price: $775
Shipping: Included in the U.S., for shipping elsewhere, please request a quote
Beer Analysis 108B
One additional six-sample pack (bottles or cans) shipped quarterly
Price: $265
Shipping: Included in the U.S., for shipping elsewhere, please request a quote
Beer Analysis 108C
Two additional six-sample packs (bottles or cans) shipped quarterly
Price: $395
Shipping: Included in the U.S., for shipping elsewhere, please request a quote
Analysis
A variety of analyses may be performed for samples, at the discretion of the laboratory performing the analysis. Recommended ASBC methods are provided for each analysis.
| Analysis | Recommended ASBC Method |
|---|---|
| Air | |
| Alcohol | Beer-4A, B, C, D, E |
| Apparent Extract | Beer-3, Beer-4E |
| Ash | Beer-13 |
| Bitterness | Beer-23A, D |
| Calcium | Beer-20A, B, C |
| Carbon Dioxide | Beer-13B |
| Color | Beer-10A, B |
| Copper | Beer-19A, B, C (Archived) |
| Diacetyl | Beer-25E |
| Dimethyl Sulfide | Beer-44 |
| Extract of Original Wort | Beer-4E, Beer-6A |
| Foam | Beer-22A, B |
| Free Amino Nitrogen | Beer-31 |
| Gluten | Beer-49 |
| Iron | Beer-18A, B, C |
| ISO-Alpha Acids | Beer-23C |
| Pentanedione | Beer-25E |
| pH | Beer-9 |
| Real Extract | Beer-5A, B, C |
| Sodium | Beer-36 |
| Specific Gravity | Beer-2A, B |
| Sulfur Dioxide | Beer-21 |
| Total Acidity | Beer-8A, B |
| Total Haze | Beer-27A, B |
| Total VDK | Beer-25A, B, C, D, E |
Hops Analysis
One hops sample per month is sent to subscribers for analysis. Three types of hops samples (powder, pellets, or extract) are sent on a rotating basis, for a total of four of each type per year.
Series
Hops Analysis 102
One sample of hop powder, pellets, or extract on a rotating basis shipped monthly
Base Price: $425
Shipping: Included in the U.S., for shipping elsewhere, please request a quote
Analysis
A variety of analyses may be performed for the hop samples, at the discretion of the laboratory performing the analysis.
Analysis
- Alpha-Acids
- Beta-Acids
- Cohumulone
- Colupulone
- Hop Storage Index
Malt Analysis
Depending upon series subscription, subscribers will receive a set quantity of two malt samples consisting of two-row and /or six-row varieties, with the additional option of also receiving standard malt samples.
Series
Malt Analysis 107E
One (1) set of two samples shipped quarterly - 8 total samples annually
Price: $395
Shipping:
- U.S. - Included
- Canada - $155
- Mexico - $200
- Elsewhere - $255
Malt Analysis 107EM
One (1) set of two samples shipped monthly - 24 total samples annually
Price: $680
Shipping:
- U.S. - Included
- Canada - $355
- Elsewhere - Request a quote
Malt Analysis 107F
Two (2) sets of two samples shipped quarterly - 16 total samples annually
Price: $580
Shipping:
- U.S. - Included
- Canada - $220
- Elsewhere - Request a quote
Malt Analysis 107FM
Two (2) sets of two samples shipped monthly - 48 total samples annually
Price: $1090
Shipping:
- U.S. - Included
- Canada - $430
- Elsewhere - Request a quote
Malt Analysis 107G
One (1) set of two samples shipped quarterly PLUS two (2) packages of standard malt per shipment - 8 total samples annually
Price: $860
Shipping:
- U.S. - Included
- Canada - $220
- Elsewhere - Request a quote
Analysis
A variety of analyses may be performed for the samples, at the discretion of the laboratory performing the analysis. Recommended ASBC methods are noted.
| Analysis | Recommended ASBC Method |
|---|---|
| Moisture % | Malt-3 |
| % Extract - Fine Grind (dry basis) | Malt-4 |
| % Extract - Course Grind (dry basis) | Malt-4 |
| % Fine-Course Difference (dry basis) | Malt-4 |
| Color of Wort, 1/2" Cell | Wort-9 |
| Diastatic Power, Salt Ext. (degree) | Malt-6 |
| Alpha-Amylase, Salt Ext. (20° units) | Malt-7 |
| % Soluble Protein in Malt (dry basis) | Wort-17 |
| % Total Protein (dry basis) | Malt-8 |
| % Soluble/Total Protein (dry basis) | |
| Screen Assortment % on 7/64" | Malt-2B |
| Screen Assortment % on 6/64" | Malt-2B |
| Screen Assortment % on 5/64" | Malt-2B |
| Screen Assortment % through 5/64" | Malt-2B |
| FAN (ppm) | Wort-12B |
| Viscosity, Absolute (cP) | Wort-13B |
| Turbidity (NTU) | |
| Test Weight | Malt-2A |
| NDMA | Malt-10 |
| Friability | Malt-12 |
| DMSP | Malt-14 |
| Deoxynivalenol | Malt-13 |
| Beta-Glucan, Wort (mg/L) | Wort-18B |
Barley Analysis
Subscribers receive two barley samples consisting of two-row and/or six-row samples of barley on a quarterly basis.
Series
Barley Analysis 106
One (1) set of two samples shipped quarterly - 8 total samples annually
Price: $395
Shipping:
- U.S. - Included
- Canada - $155
- Mexico - $200
- Elsewhere - $255
Analysis
A variety of analyses may be performed for the samples, at the discretion of the laboratory performing the analysis. Recommended ASBC methods are noted.
| Analysis | Recommended ASBC Method |
|---|---|
| Moisture, % | Barley-5A, B, C |
| Protein, dry basis, % | Barley-7A, B, C |
| Plump % on 6/64" | Barley-2C |
| Plump % on 5/64" | Barley-2C |
| Plump % Thin thru 5/64" | Barley-2C |
| Germinative Energy (24 hours), % | Barley-3A |
| Germinative Energy (48 hours), % | Barley-3A |
| Germinative Energy (72 hours), % | Barley-3A |
| Germinative Capacity (48 hours), % | Barley-3B |
| Skinned & Broken Kernels, % | Barley-2F |
| Water Sensitivity, % | Barley-3C |
| Test Weight, lb/bu | Barley-2B |
| Injury by Sprout, % | Barley-2H |
| Deoxynivalenol, ppm | Barley-11 |
Mycotoxins Analysis
With Fusarium head blight posing a real threat to the barley crop, ASBC members and others using or processing malt are concerned with the possible presence of deoxynivalenol (also known as DON or vomitoxin) in barley, malt, and brewed products. AACC, which shares headquarters with ASBC, offers a quarterly check sample series for mycotoxins, designated as MYCO in the AACC Laboratory Proficiency Rating Program. This sample is offered to ASBC members through the AACC Laboratory Proficiency Rating Program.
Series
Samples of mixed, ground grains are naturally (but heavily) contaminated with analyzable levels of aflatoxin, deoxynivalenol, and fumonisin. Four different samples, varying in levels of contamination, are sent to subscribers on a quarterly basis.
Mycotoxins Analysis MYCO
Mycotoxins, including aflatoxin, deoxynivalenol (vomitoxin), and fumonisin shipped quarterly
Price: $925
Shipping:
- U.S. - $60
- Canada - $240
- Elsewhere - Request a quote