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Display Title

A-103: Profiling the shelf life and shelf stability of hop and malt driven beers using SBSE-TD-GC-MS/O and trained sensory panel evaluation

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E. Brown (1), A. Duffy (1), S. Cohen (1), B. TAUBMAN (1), D. Sedin (2); (1) Appalachian State University, Boone, NC, U.S.A.; (2) New Belgium Brewing Company, Fort Collins, CO, U.S.A.

Poster

The purpose of this joint study between Appalachian State University and New Belgium Brewing Company was to identify active aroma compounds of a hop-driven and a malt-driven beer to understand the impact of storage conditions, particularly duration and temperature, on beer aroma character. This was achieved by developing an analytical method in conjunction with a trained descriptive panel, which identified a list of aroma attributes relevant to this study by evaluating a series of beers ranging from 14 to 90 days old, and difference testing focused on aromas defined by the descriptive panel to evaluate attributes central to the character profiles of the beers during storage. Stir bar sorptive extraction (SBSE) on an ethylene glycol-bonded phase (EG) was used to concentrate analytes based on broad interactions with both polar and nonpolar matrices in the media. Thermal desorption-gas chromatography-mass spectrometry coupled with olfactometry (TD-GC-MS/O) was used to identify analytes of interest. Preliminary results from the GC-MS data suggest a synergistic effect among various compounds results in overall sensory changes with respect to storage time and temperatures. These results are consistent with descriptive panel data that identified unique aroma characteristics for each beer as they were aged under different storage conditions. However, the sensory data indicate that storage temperature had a minor impact on beer aroma throughout the aging process and was variable between beer styles. Overall, this work will provide a tool the brewery quality control lab may use to monitor and predict the effects of aging and identify process variables that can be altered to improve shelf life and stability. Future work will focus on development of a rapid screening protocol and broadening the applicability of these methods.

Brett Taubman is a faculty member of the A. R. Smith Department of Chemistry at Appalachian State University (ASU), where he is engaged in instruction and academic research within the chemistry and fermentation sciences. He has earned B.S. degrees in both finance and chemistry from the Pennsylvania State University and Montana State University, respectively, and a Ph.D. degree in analytical and environmental chemistry from the University of Maryland (2004). Following his graduate studies, he worked as a post-doctoral research associate at the Pennsylvania State University before joining the chemistry faculty at ASU in 2007. Brett has successfully developed a pilot instructional brewing facility on the ASU campus and currently serves as president of Ivory Tower, Inc., a 501(c)(3) nonprofit corporation with the mission of supporting research and education within the fermentation sciences. He helped to develop the four-year degree program in fermentation sciences and shares time between that program and the Chemistry Department. He has been brewing and teaching brewing sciences and technology for more than 10 years and is a member of the American Society of Brewing Chemists, Master Brewers Association of the Americas, and Institute of Brewing and Distilling.

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