P-19

Beta-glucan content and endo-betaglucanase activities of individual malted barley grains.
ROBERTA MARINS DE SÁ and G. H. Palmer. International Centre for Brewing and Distilling, Heriot Watt-University, Riccarton, Edinburgh, EH14 4AS, Scotland.

Cell wall modification (beta-glucan breakdown) is regarded as a key step in extract development during malting and brewing. It has been suggested that the rate of modification, of the grains of a barley sample, is principally determined by their contents of cell wall beta-glucan and their potential to synthesise beta-glucanase. Therefore, malt samples, which contain low beta-glucan levels and high beta-glucanase activities, are considered suitable for brewing. However, traditional malt analyses do not detect the homogeneity of modification of the grains of a sample of malt. The aims of this study were to (a) assess the distribution of beta-glucan content and endo-betaglucanase activity in individual grains of barley and malt and (b) compare the degree of physical modification of single grains of malt with their corresponding levels of beta-glucan. Barley variety Decanter was malted and samples were collected after 24, 48, 72 and 96 hours of germination. Samples were analysed for their total beta-glucan content and beta-glucanase activity, according to the McCleary Method and the Azo-Barley Glucan Method, respectively. These methods were later adapted in order to evaluate single grains. The degree of physical modification and beta-glucan content were analysed in kilned malt; corresponding beta-glucanase activity was analysed using (unkilned) green malt. The distribution of beta-glucan content (mg/grain), beta-glucanase activity (U/grain) and degree of modification in each sample will be presented. Malt samples showed a wide distribution of the content of beta-glucan and beta-glucanase activity in individual grains. Total beta-glucan of the whole sample gave no indication of the differences in beta-glucan content in individual grains and did not correlate with the variation of physical modification that occurred in individual grains. This also applied to beta-glucanase activity. A weak correlation between beta-glucan content of individual malt grains and endo-betaglucanase activity was observed, indicating that other factors may be involved in controlling the rate of beta-glucan breakdown and endosperm modification during malting. These results showed that total beta-glucan content or total beta-glucanase activity of malt samples are not the best indicators of overall modification of the endosperm. The results of this study show that significant variations in levels of beta-glucan and beta-glucanase can occur in the individual grains of a barley sample during malting. Although beta-glucan breakdown is important, there are complimentary factors, which control the overall rate at which the endosperm is modified during malting.

Roberta Marins de Sá is a second year PhD student at the International Centre For Brewing and Distilling (ICBD), under the supervision of Professor G. H. Palmer. She is sponsored by Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq), Brazil. She previously received an MSc. in Food Science from UFSC (Brazil). Her research interests centre on the study of barley and malt. At present she is engaged in detailed examination of the physiological relationship between endo-betaglucanase activity, beta-glucan breakdown and the overall physical modification of the endosperm during malting.

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