P-16

Real-time RT-PCR detection of beer-spoilage lactic acid bacteria.
RIIKKA JUVONEN, Tiina Partanen, Auli Haikara, and Teija Koivula. Technical Research Centre of Finland, Biotechnology, P.O. Box 1500, FIN-02044 VTT, Finland.

Reverse transcriptase PCR (RT-PCR) is a potentially sensitive, specific and rapid in vitro technique for amplification of ribonucleic acid (RNA) molecules. RT-PCR could also allow specific detection of viable cells, since RNA is generally less stable in dead cells than DNA. Recently, the development of real-time PCR technology has greatly facilitated the PCR analysis, making simultaneous amplification, detection and quantification of target nucleic acid molecules possible. Here we report the application of real-time RT-PCR for the detection of RNA in beer-spoilage lactic acid bacteria (LAB) belonging to species Lactobacillus brevis, Lactobacillus lindneri and Pediococcus damnosus. Moreover, various methods were compared and optimised for the isolation of RNA. Elongation transcription factor messenger RNA (Ef-Tu mRNA) and ribosomal RNA (rRNA), which are abundantly and constitutively expressed by metabolizing bacterial cells, were used as primer targets. The species and group specific primers were previously published or designed in the course of the study. The amplification and detection of amplicons was carried out using a one-step RT-PCR kit, SyBrGreen chemistry and a capillary-based LightCycler instrument that allows ultra-rapid thermal cycling. A conventional RNA extraction method based on mechanical disruption of cells in the presence of a chaotropic agent and a total RNA isolation kit from Qiagen both produced reasonable yields of good-quality RNA from LAB. In optimal magnesium concentration, the RT-PCR assays for rRNA and Ef-TU mRNA were able to detect 2-6 fg and 2-6 ng purified RNA per reaction, respectively. The initial RNA concentrations correlated well with the onset of exponential amplification (Cp values; r > -0.98) over 3-8 log-units, confirming the suitability of the technology for RNA quantification. The reproducibility of Cp values was good. Preliminary experiments with beer indicated that the assays could be used to detect the contamination of beer by LAB. The target RNAs were still detectable in killed lactobacilli cells three weeks after a mild heat-treatment. Experiments to study the degradation of cellular RNA after other killing treatments are on-going. The use of a rapid-cycle real-time format simplifies and speeds up the RT-PCR analysis and reduces the risk for false positive PCR results. Further improvements, especially in the sample treatment step, are needed before the methodology can be implemented in a brewery QC laboratory.

Riikka Juvonen received a MSc in Food Microbiology from the University of Helsinki in 1997. She began employment with Technical Research Centre of Finland in 1995 as a trainee. After her graduation she received a position as a research scientist and was focusing on the rapid detection of beer-spoilage organisms. Since then, she has functioned as a project leader and participated in several national and international project. She has received supplementary courses, e.g., on nucleic acid sequence analyses, molecular biological and microscopical techniques, project management and communication skills. She is currently working on her PhD degree.

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